ASTM D5896-1996(2007) 纤维素材料碳水化合物分配的标准试验方法
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【英文标准名称】:StandardTestMethodforCarbohydrateDistributionofCellulosicMaterials
【原文标准名称】:纤维素材料碳水化合物分配的标准试验方法
【标准号】:ASTMD5896-1996(2007)
【标准状态】:现行
【国别】:
【发布日期】:1996
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D01.36
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:纤维素;色谱法;水解;单糖;纸浆;试验
【英文主题词】:carbohydrate;carbohydratedistribution;chromatography;distribution;hemicellulose;hydrolysis;ionchromatography;monosaccharides;PAD;sugars
【摘要】:Thistestmethodrequirestotalhydrolysisofcarbohydratematerialtomonosaccharides,andisthusapplicabletoanycellulosicorrelatedmaterialthatundergoessubstantialhydrolysis,includingcellulosederivativessuchascelluloseacetate.Thecarbohydratecompositionofacellulosicmaterialcanbeexpressedonthebasisofthetotalinitialsample,oronthebasisofthecarbohydrateportionofthesample.Theformerrequiresquantitativehandlingandmayrequirespecialknowledgeoftheothercomponentspresentinordertoestablishtheabsolutecarbohydratelevelordetermineindividualwoodhemicellulosessuchasgalactoglucomannan,etc.Sincethesolidportionofpurifiedpulpsisalmostallcarbohydrate(98+%),thelatterbasisisoftenusedtoexpressthecarbohydratedistributionasapercent.Ifheatedunderalkalineconditions,isomericsugarsmaybegintoappearinthechromatogram.Themajorimpuritypresentinpurifiedpulpsissaccharinicacids.Theseacidiccomponents,andotheranionssuchassulfate,carbonate,andacetateareremovedbyastrongbaseanionexchangeSPE,andwouldneedtobedeterminedseparatelytogetamoreexactcarbohydratedistribution.1.1Thistestmethodcoversthedeterminationofthecarbohydratecompositionofcellulosicmaterialssuchasgroundwoodmeal,chemicallyrefinedpulp,mechanicalpulps,brownstocks,andplantexudates(gums)byionchromatography.Thistestmethodissuitableforrapid,routinetestingoflargenumbersofsampleswithhighaccuracyandprecision.Forareviewofthistechnique,seeLee(1).1.2ThevaluesstatedinSIunitsaretoberegardedasstandard.Nootherunitsofmeasurementareincludedinthisstandard.Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.Forhazardstatement,seeSection8.
【中国标准分类号】:Y30
【国际标准分类号】:71_040_50;85_040
【页数】:3P.;A4
【正文语种】:
【原文标准名称】:纤维素材料碳水化合物分配的标准试验方法
【标准号】:ASTMD5896-1996(2007)
【标准状态】:现行
【国别】:
【发布日期】:1996
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D01.36
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:纤维素;色谱法;水解;单糖;纸浆;试验
【英文主题词】:carbohydrate;carbohydratedistribution;chromatography;distribution;hemicellulose;hydrolysis;ionchromatography;monosaccharides;PAD;sugars
【摘要】:Thistestmethodrequirestotalhydrolysisofcarbohydratematerialtomonosaccharides,andisthusapplicabletoanycellulosicorrelatedmaterialthatundergoessubstantialhydrolysis,includingcellulosederivativessuchascelluloseacetate.Thecarbohydratecompositionofacellulosicmaterialcanbeexpressedonthebasisofthetotalinitialsample,oronthebasisofthecarbohydrateportionofthesample.Theformerrequiresquantitativehandlingandmayrequirespecialknowledgeoftheothercomponentspresentinordertoestablishtheabsolutecarbohydratelevelordetermineindividualwoodhemicellulosessuchasgalactoglucomannan,etc.Sincethesolidportionofpurifiedpulpsisalmostallcarbohydrate(98+%),thelatterbasisisoftenusedtoexpressthecarbohydratedistributionasapercent.Ifheatedunderalkalineconditions,isomericsugarsmaybegintoappearinthechromatogram.Themajorimpuritypresentinpurifiedpulpsissaccharinicacids.Theseacidiccomponents,andotheranionssuchassulfate,carbonate,andacetateareremovedbyastrongbaseanionexchangeSPE,andwouldneedtobedeterminedseparatelytogetamoreexactcarbohydratedistribution.1.1Thistestmethodcoversthedeterminationofthecarbohydratecompositionofcellulosicmaterialssuchasgroundwoodmeal,chemicallyrefinedpulp,mechanicalpulps,brownstocks,andplantexudates(gums)byionchromatography.Thistestmethodissuitableforrapid,routinetestingoflargenumbersofsampleswithhighaccuracyandprecision.Forareviewofthistechnique,seeLee(1).1.2ThevaluesstatedinSIunitsaretoberegardedasstandard.Nootherunitsofmeasurementareincludedinthisstandard.Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.Forhazardstatement,seeSection8.
【中国标准分类号】:Y30
【国际标准分类号】:71_040_50;85_040
【页数】:3P.;A4
【正文语种】:
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